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Diesel
Fuel Analysis
Fuel analysis has become a very important part
of all maintenance and purchasing functions. The cost of diesel fuel,
although expensive, is small when compared to the problems that may
develop without the proper purchase specifications, verification of
those specifications, handling, storage and distribution. Generally
speaking, most fuel is within the grade; however, on occasion a fuel
delivery may be substandard. Fuel will also degrade and become contaminated
in storage and transfer. It is almost impossible to retrace the sequence
of events leading up to fuel problems unless an accurate record of
the quality of the fuel is maintained. This can only be done by periodic
laboratory analysis of the fuel.The properties of commercial fuel
oils depend on the refining practices employed and the nature of the
crude oils from which they are produced. Distillate fuel oils, for
example, may be produced within the boiling range of 150 and 400 degrees
centigrade (300 and 755 degrees Fahrenheit), having many possible
combinations of various properties such as volatility, ignition quality,
viscosity, and other characteristics.

Receipt Inspections / Quality Control
As a rule, all fuel deliveries should be sampled and tested. The economics
of sampling are not only to guarantee the money paid to the supplier
was well spent, but also to ensure the integrity of your entire system
against unplanned downtime. This fuel delivery could, if contaminated
or "off grade," cause enormous problems when mixed with
the fuel you already have in the tank.
It is wise to arrange in critical applications a system whereby you
have the opportunity to sample and test the fuel prior to introducing
the fuel into your primary tank(s). This can be done by having the
tanker truck leave the trailer on-site until you have completed your
testing, or by building a holding tank to accept deliveries for analysis
prior to dispensing into your storage tanks.
Sampling Storage Tanks
Periodic sampling and inspection of stored fuel will reveal several
important quality parameters that if gone undetected may cause unnecessary
problems in the operation of the diesel generator. During long-term
storage of diesel fuel, water, sludge, and microorganisms will accumulate.
The early detection of these contaminates will eliminate fuel related
problems later on.
Sampling Techniques
As with any sampling program, a representative and accurate sample
is necessary to receive the full benefit of the analysis. The reasons
to sample may differ; therefore, the sampling methods will be different.
In order to evaluate the concentration of sludge, water, and debris
on the bottom of the tank, you will want to take a sample at the lowest
point in the system. This sounds easier than it is, since in many
situations, the fill tube is the only access to the tank.
This causes a situation where, when the tank is filled, the velocity
of the filling action washes this area clean of debris, and you are
unable to get to the areas beyond the fill pipe. A long sample tube
strapped to PVC pipe and angled to the side may be of help. If this
is not the situation, a simple bottom sampler will normally suffice.
When a sample of fuel for general quality testing is required, a middle
and bottom composite will usually suffice.
When fuel has been received in good condition and contamination and
degradation are the only reason for sampling, you may not require
all of the tests that were performed on the original load. An example
of testing that is not required would be sulfur, viscosity, cetane,
and distillation. If the fuel in storage proves to have no contamination
and the stability is acceptable, these values would not change.
ASTM D-975 Specifications
ASTM Specification D-975 for diesel fuel oils is intended as a statement
of permissible limits of significant fuel properties used for specifying
the wide variety of commercially available diesel fuel oils. Limiting
values of significant properties are prescribed for three grades of
diesel fuel oils. These grades and their general applicability of
use in diesel engines are broadly indicated as follows:
Grade No. 1-D comprises the class of volatile fuel oils from
kerosene to the intermediate distillates. Fuels within this grade
are applicable for use in high-speed engines in services involving
frequent and relatively wide variations in loads and speeds, and also
for use in cases where abnormally low fuel temperatures are encountered.
Grade No. 2-D includes the class of distillate gas
oils of lower volatility. These fuels are applicable for use in high-speed
engines in services involving relatively high loads and uniform speeds,
or in engines not requiring fuels having the higher volatility or
other properties specified for Grade No. 1-D.
Grade No. 4-D covers the class of more viscous distillates
and blends of these distillates with residual fuel oils. These fuels
are applicable for use in low and medium-speed engines employed in
services involving sustained loads at substantially constant speed.
For more information contact Herguth or call 1-888-HERGUTH (437-4884) |
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